Table of Contents

Preface xv

Acknowledgments xvii

THIN FILMS (MICROELECTRONICS, HTSC)

The Texture of Thin Nisi Films and Its Effect on Agglomeration 3
K. De Keyser, C. Detavernier , R. L. Van Meirhaeghe, J. Jordan-Sweet, and C. Lavoie

Epitaxial Substrates from Ni-Based Ternary Alloys With Cr and W 11
D.P. Rodionov, I.V. Gervasyeva, Yu.V. Khlebnikova, and V.A. Kazantsev

Cube Texture Formation in Ni-Pd and Ni-Pd-W Alloys For HTS Tapes 23
I.V. Gervasyeva, D.P. Rodionov, Yu.V. Khlebnikova, G.A. Dosovitskii, and A.R. Kaul

Texture of Rapidly Solidified Cu Thin Films Studied by SEM EBSD and TEM 35
R. Zhong, A. Kulovits, J.M.K. Wiezorek, and J.P. Leonard

Control of Texture in Polycrystalline Thin Films Used as Data Storage Media 47
David E. Laughlin, Hua Yuan, En Yang, and Chun Wang

Influences of Processing Parameters on Microstructures and Microtextures of Au Flip Chip Bonds During Microelectronics Packaging 57
P Yang, C-M Li, D-M Liu, M Hung, M Li, and W-M Mao

TEXTURE AT NON-AMBIENT CONDITIONS

In Situ Observation of Texture Evolution in Ti-10-2-3 65
Seerna L. Raghunathan, Richard Dashwood, Martin Jackson, Sven Vogel, and David Dye

Study of Texture Evolution at High Strain Rates in FCC Materials 73
Nilesh Gurao, Satyam Suwas, and Rajeev Kapoor

Texture and Microstructure Development in Copper after Cryogenic Rolling and Heat Treatment 83
A. Haldar, D. Das, and P.P. Chattopadhyay

In-Situ EBSD Study of the a-y-a Phase Transformation in a Microalloyed Steel 95
Lischewski, D. M. Kirch, A. Ziemons, and G. Gottstein

Texture Changes during Phase Transformations Studied In Situ With Neutron Diffraction 103
Hans-Rudolf Wenk

NOVEL TEXTURE MEASUREMENT TECHNIQUES INCLUDING 3D

Three-Dimensional FIB-OIM of Ceramic Materials 117
Shen J. Dillon and Gregory S. Rohrer

Comparison of X-Ray and EBSD Textures for Back-Annealed AI-Mg Alloys 125
0. Engler

A New Method for Quantification of Texture Uniformity of Plate 135
Peter Jepson and Robert Bailey

Separating Coincident Electron Backscatter Diffraction Patterns Near Interfaces 147
Josh Kacher, Brent L. Adarns, David Fullwood, and Colin Landon

Rapid Texture Determination Based on Two Dimensional X Ray Detector 155
Weimin Mao

Semiautomatic Determination of Orientations and Elastic Strain from Kossel Microdiffraction 163
Adam Morawiec, Raphael Pesci, and Jean-Sebastien Lecomte

Statistically Reliable EBSD Analysis Method of Grain Boundary Characterization 171
D.H. Kim, J.Y.Kang, D.I. Kim, E.K. Her, S.J. Kim, H.N. Han, K.H. Oh, and H.C. Lee

3D Microstructures and Textures of a Plane Strain Compressed (1 10}4 12> AI-0.3% Mn Single Crystal 181
H. Paul, J.H. Driver, and CI. Maurice

Three Laws of Substructure Anisotropy of Textured Metal Materials, Revealed by X-Ray Method of Generalized Pole Figures 189
Yuriy Perlovich, Margarita Isaenkova, and Vladimir Fesenko

3D-Microstructural and Texture Characterization in Different Length Scales 197
Roumen Petrov and Patricia Gobernado Hernandez, Orlando Leon Garcia, Hemant Sharma, and Leo Kestens

Local Crystal Rotations of Bulk Grains by High-Resolution EBSD during Hot PSC of AI-0.1 % Mn Polycrystals 205
Romain Quey, David Piot, and Julian Driver

Grain Boundary Orientations in a Fe-Mn-Cu Polycrystalline Alloy 213
M. Takashima and P. Wynblatt

Development of a TEM-Based Orientation Microscopy System 221
S. Zaefferer and G. Wu

COMPLEX OXIDES AND OTHER COMPOUNDS

Domain Control Effect on Voltage-Strain in BaTi03 Single Crystal 231
Yoshio Akimune, Kazuo Matsuo, Ryutaro Oishi, and Akira Okada

Tentative Simulation of Crystal Rotation for NaCl Structures 239
Hiroaki Masui

INTERFACE TEXTURES

Grain Boundary Patterns in Dynamically Recrystallized Quartz Aggregates 251
Cristiane Castro and Leonardo Lagoeiro

The Correlation between Grain Boundary Character and lntergranular Corrosion Susceptibility of
2124 Aluminum Alloy 261
L. H. Chan, H. Weiland, S. Cheong, G.S. Rohrer, and AD. Rollett

Rodrigues-Frank Spaces for Misorientations and Orientation Relationships between Crystals of Any Two Crystallographic Point Groups 269
Youliang He and John J. Jonas

Origins of Texture Memory in Steels 281
Bevis Hutchinson and Leo A.I. Kestens

A Grain Boundary Analysis of Cemented Tungsten Carbides using OIM 291
Vineet Kumar, Zhigang Zak Fang, S.I. Wright and M.M. Nowell

The Effect of Grain and Phase Boundary Misorientation on Nucleation during Solid-state Phase Transformations in a Co-l5Fe Alloy 305
H. Landheer, S.E. Offerman, and L.A.I. Kestens, T. Takeuchi, M. Enomoto, and Y. Adachi

Microstructural Modification in a 150-1 5Ni-2.2 Mo-Ti Modified Austenitic Stainless Steel through Twin Induced Grain Boundary Engineering 313
Sumantra Mandal, P.V. Sivaprasad, and V. Subramanya Sarrna

Effect of Strain Path and Annealing on Development of Resistance to lntergranular Degradation in Austenitic Stainless Steels 323
V. Randle, R. Jones, T.J. Marrow, and D. Engelberg

Evolution of the Grain Boundary Character Distribution in Strontium Titanate during Grain Growth 335
Herbert M. Miller and Gregory S. Rohrer

A Model for the Origin of Anisotropic Grain Boundary Character Distributions in Polycrystalline Materials 343
Gregory S. Rohrer, Jason Gruber, and Anthony D. Rollett

Nucleation of the Primary A1 Phase on TiA13 during Solidification of a Hot-Dip Zn-1 1% A1-3%Mg-On2%SCi oating on Steel Sheet 355
Kazuhiko Honda, Kohsaku Ushioda, and Wataru Yamada

RECRYSTALLIZATION TEXTURE: RETROSPECTIVE VERSUS CURRENT PROBLEMS

Textural lnhomogeneity Effect during the Monte Carlo Simulation of the Abnormal Goss Grain Growth in Fe-3%Si Steel Grade HiB 365
T. Baudin, R. Penelle, and D. Ceccaldi

Avoiding Roping and Ridging in AA6XXX Sheets: Characterizing the Initial State 373
T.A. Bennett, R.H. Petrov, and L.A.I. Kestens

Development of Cube Texture in Cold-Rolled and Annealed Multilayer Tapes for Coated Superconductor Applications 381
P.P. Bhattacharjee and R.K. Ray

Effects of Elastic Modulus on Deformation and Recrystallization of High Purity Nb 391
D. Baars, H. Jiang, T.R. Bieler, A. Zamiri, F. Pourboghrat, and C. Compton

Through-Process Texture Modeling of AA6016 from Hot Rolling to Final Annealing 399
C. Bollmann and G. Gottstein

Cube Texture Due to Dynamic Recrystallization in Pb and Pb-62%Sn Alloys under Equal Chanel Angular Extrusion Processing 409
R.E. Bolmaro, V.L. Sordi, M. Ferrante, WeiMin Gan, and H.-G. Brokmeier

Annealing Texture Evolution 421
I.L. Dillamore

On the Stability of Recrystallization Textures in Low Alloyed Zirconium Sheets 429
FranCois Gerspach, Nathalie Bozzolo, and Francis Wagner

An Analysis of the Texture and Mean Orientation of Aluminium Alloy AA5052 Subjected to Forward and Reverse Hot Torsion and Subsequent Annealing 437
0. Hernandez-Silva, B.P. Wynne, and W. M. Rainforth

Evolution of { l l l } Recrystallization Texture in Al-Mg-Si Alloy Sheets Processed by Symmetric and Asymmetric Combination Rolling 445
Hirofumi Inoue, Satoshi Kobayashi, Masayuki Hori, Toshio Komatsubara, and Takayuki Takasugi

Effect of External Constraint and Deviation from Ideal Orientation on Development of Rolling Texture in Pure Aluminum Single Crystal Having {loo} Orientation 453
Keizo Kashihara and Hirosuke lnagaki

Nucleation and Growth of New Grains in Deformed Quartz Single Crystals 461
Leonardo Lagoeiro and Paola Barbosa

Rolling and Annealing Textures of Silver Sheets 469
Dong Nyung Lee, Heung Nam Han, and Se-Jong Kim

Function of Layer Thickness on the Microstructural Evolution in Copper of Annealed Roll-Bonded CuNb Composites 481
S.C.V. Lim and A.D. Rollett

Influence of Taylor Factor M on Recrystallization of The Cube and Cube-Family Grains in FCC Metal 489
Hiroaki Masui

Multi-Cycle Pinch Welding of 304L Tubes: lnhomogeneities in Deformation and Recrystallization Textures and Microstructures 499
C.T. Necker, A.N. Marchi, and M.G. Smith

Effect of Mg Concentration on Texture Formation in AI-Mg Alloys during High Temperature Compression 507
Kazuto Okayasu, Hiroki Takekoshi, Masayuki Sakakibara, and Hiroshi Fukutomi

Ultra-Fine Grain Austenitic Stainless Steels: Influence of Texture during Recrystallization 515
Angeline Poulon-Quintin, Stephanie Brochet, Jean-Bernard Vogt, Jean-Christophe Glez, and Jean-Denis Mithieux

Patterns of Deformation and Associated Recrystallization in Warm/Hot Deformed AA6022 523
S. Raveendra, S. Mishra, H. Weiland, and I. Samajdar

Studies on Texture and Microstructure of Cryorolled and Annealed Cu-5%AI, Cu-5%Zn Alloys 529
V.L. Niranjani, Nilesh Gurao, U. Wendt, S. Suwas, and V. Subramanya Sarma

Modeling of Texture Development during Tandem Hot Rolling of AA3 1 03 537
C. Schafer, V. Mohles, and G. Gottstein

Texture Modification in Asymmetrically Rolled Aluminum Sheets 547
Jurij Sidor, Roumen Petrov, Alexis Miroux, and Leo Kestens

In-Situ SEM/EBSP Analysis during Annealing in AI-Mg Alloys 555
Yoshimasa Takayama, Kazuhiro Morita, Hajime Kato, and Yoshimasa Ookubo

Oriented Grain Growth and the Effect of In-Situ Annealing on Texture in AlMn Alloys 561
Caterina E. Tommaseo and H. Klein

Subgrain Coarsening of Hot-Rolled AA5005 Aluminum Alloy: A Comparison between EBSD Observations and Monte Carlo 569
Shengyu Wang, Mohammed H. Alvi, and Anthony D. Rollett

Influence of Low Angle Grain Boundaries on Recrystallization 577
Myrjam Winning and Dierk Raabe

BIOMATERIALS

Comparison of Calcite Crystallographic Texture in the Shells of the Rhynchonelliform Brachiopod, Terebratulina Retusa and the Bivalve Mollusc, Mytilus Edulis 587
M.Cusack, A. Perez-Huerta, P. Dalbeck, P. Chung, and M.R. Lee

Wear Resistance and Texture Evolution of Ultra High Molecular Weight Polyethylenes during Uniaxial Compression 595
D.S. Li, H. Garmestani, S.C. Davis, L.K. Moss, A.K. Siddiqi, J.B. Guthrie, N. Johansen, and L. Matrisciano

Texture and Microstructure of Modern Rhynchonellide Brachiopod Shells-An Ontogenetic Study 605
E. Griesshaber, R.D. Neuser, U. Brand, and W.W. Schmahl

Peering Into the Eyes of Trilobites using EBSD 619
C. Torney, M.R. Lee, and A.W. Owen

Texture and Anisotropy of MP35N Wire for Conduct Leads 627
Bernard Q. Li and Tom Steigauf

Crystallographic Textures from the Exoskeleton of the Lobster Hornarus Arnericanus and Calculation of the Mechanical Properties of the Calcite Phase 637
L. Raue, H. Klein, D. Raabe, and H. Fabritius

TEXTURE EFFECTS ON DAMAGE ACCUMULATION

Experimental Characterization of the Effect of Crystallography on the Three Dimensional Nucleation and Growth of Fatigue Cracks in Metals 657
J-Y. Buffiere, E. Ferrie, H. Proudhon and W. Ludwig

Reversible Texture Transition during Accumulative Roll Bonding 669
Naoya Kamikawa, Xiaoxu Huang, Grethe Winther, Nobuhiro Tsuji, and Niels Hansen

Evolution of Grain Boundary Microstructures in Molybdenum by Thermomechanical Processing from Single Crystals 681
Shigeaki Kobayashi, Sadahiro Tsurekawa, and Tadao Watanabe

Local Characterization of Void Initiation on IF Steel by FIB-EBSD Technique 693
Orlando Leon-Garcia, Roumen Petrov, and Leo Kestens

Experimental and Simulation Study on Texture and Bendability of AA5XXX Aluminum Alloys 701
Y. Liu, Z. Long, X. Y . Wen, S. Ningileri, and S. K Das

Some Aspects on Grain Growth in ECAP Deformed and Heat Treated Aluminum 1.2% Hafnium Alloy 709
0. Al-Buhamad, M.Z. Quadir, and M. Ferry

Kinetic Measurements of Texture and Microstructural Evolution using Orientation Distribution Function and Residual Stress Relaxation 717
S. Saimoto, J. Cooley, and C. Gabryel

Texture and Micro-Hardness Evolution of Submicrograined Copper 725
X. S. Yao, Y . D. Liu, Q. W. Jiang, X. Zhao, and L. Zuo

DIGITAL MICROSTRUCTURES

A Model of Plastic Spin Taking into Account Grain Interaction During Rolling 735
A. Fourty, J.W. Signorelli, and R.E. Bolmaro

CPFEM Investigation of the Effect of Grain Shape on the Planar Anisotropy and the Shear Banding of Textured Metal Sheets 745
Laurent Delannay, Maxime A. Melchior, Anand K. Kanjarla, Paul Van Houtte, and Javier W. Signorelli

Modelling of Primary Recrystallization using Digital Microstructures 757
R.E. Loge, M. Bernacki, H. Resk, H. Digonnet, Y . Chastel, and T. Coupez

Two-Phase Microstructure Generation in 3D Based on 2D Sections of a Nickel Alloy 771
C.G. Roberts, S.L. Semiatin, and A.D. Rollett

Evolution of Local Damage Variable and Its Rate of Strain-Softening Material in Tension Based on Nonlocal Theory 779
X. B. Wang

Grain Interaction and Related Elastic Fields at Triple Junction in Low Deformed IF Steel: Micromechanical Model and Reconstruction from EBSD Orientation Data 787
A.A. Zisman, V.V. Rybin, M. Seefeldt, S. Van Boxel, and P. Van Houtte

Gradient Matrix Method to Image Crystal Curvature with Discrete Orientation Data: Case Study of Triple Junction in Deformed IF Steel 803
A.A. Zisman, M. Seefeldt, S. Van Boxel, and P. Van Houtte

Author Index 815

About the Author

A.D. Rollett obtained an M.A. in Metallurgy and Materials Science from Cambridge University, England in 1977 and a Ph.D. in Materials Engineering from Drexel University in 1987. He worked for the Los Alamos National Laboratory for sixteen years, rising to be the Deputy Director of the Materials Science & Technology Division in 1994. He then moved to Carnegie Mellon University to be the Department Head in Materials Science & Engineering until 2000. He is active in the Materials Research Science & Engineering Center at CMU and is the Focal Area Point of Contact for Computational Chemistry & Materials for the DoD.