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Principles and Practice of ­Variable Pressure / ­Environmental Scanning ­Electron Microscopy ­(VP-ESEM)
RMS - Royal Microscopical Society

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Format
Hardback, 234 pages
Published
United States, 13 August 2019

Von ausführlichen Literaturhinweisen über die technischen Voraussetzungen der Rasterelektronentunnelmikroskopie geht der Text zur Beschreibung der Objektvorbereitung über. Die Kapitel im Hauptteil behandeln das Thema aus jeweils verschiedenen Fachgebieten: Physik, Materialwissenschaft, Biowissenschaften, industrielle Produktion von Lebensmitteln oder Kosmetika. Auch interdisziplinäre Ansätze werden beleuchtet.


Contents Chapter 1 -A brief historical overview 1.1 Scanning electron microscopy 1.2 The development of imaging in a gas environment Chapter 2 -Principles of SEM 2.1 Introduction 2.2 Electron sources 2.3 Electron optics 2.4 Signals and detection 2.5 Practical aspects of electron beam irradiation 2.6 the sem in operation Chapter 3 -General principles of VP-ESEM: utilising a gas 3.1 Introduction 3.2 VP-ESEM instrumentation 3.3 Signal generation in a gas 3.4 Imaging with water vapour Chapter 4 -Imaging and analysis in the VP-ESEM: the influence of a gas 4.1 Introduction 4.2 Background to theoretical calculations 4.3 Which gas? 4.4 Exploring the gas path length 4.5 How much gas? 4.6 X-ray microanalysis in the VP-ESEM Chapter 5 -Imaging uncoated specimens in the VP-ESEM 5.1 Introduction 5.2 Electronic structure 5.3 Factors affecting secondary electron emission 5.4 The influence of the specimen on the system 5.5 Time- and temperature-dependent effects 5.6 imaging soft materials 5.7 Effects of ions on imaging 5.8 Imaging with a gas: summary Chapter 6 -A lab in a chamber - in situ methods in VP-ESEM and other applications 6.1 Introduction 6.2 Nanocharacterisation of insulating materials 6.3 In situ experiments 6.4 Other applications

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Product Description

Von ausführlichen Literaturhinweisen über die technischen Voraussetzungen der Rasterelektronentunnelmikroskopie geht der Text zur Beschreibung der Objektvorbereitung über. Die Kapitel im Hauptteil behandeln das Thema aus jeweils verschiedenen Fachgebieten: Physik, Materialwissenschaft, Biowissenschaften, industrielle Produktion von Lebensmitteln oder Kosmetika. Auch interdisziplinäre Ansätze werden beleuchtet.


Contents Chapter 1 -A brief historical overview 1.1 Scanning electron microscopy 1.2 The development of imaging in a gas environment Chapter 2 -Principles of SEM 2.1 Introduction 2.2 Electron sources 2.3 Electron optics 2.4 Signals and detection 2.5 Practical aspects of electron beam irradiation 2.6 the sem in operation Chapter 3 -General principles of VP-ESEM: utilising a gas 3.1 Introduction 3.2 VP-ESEM instrumentation 3.3 Signal generation in a gas 3.4 Imaging with water vapour Chapter 4 -Imaging and analysis in the VP-ESEM: the influence of a gas 4.1 Introduction 4.2 Background to theoretical calculations 4.3 Which gas? 4.4 Exploring the gas path length 4.5 How much gas? 4.6 X-ray microanalysis in the VP-ESEM Chapter 5 -Imaging uncoated specimens in the VP-ESEM 5.1 Introduction 5.2 Electronic structure 5.3 Factors affecting secondary electron emission 5.4 The influence of the specimen on the system 5.5 Time- and temperature-dependent effects 5.6 imaging soft materials 5.7 Effects of ions on imaging 5.8 Imaging with a gas: summary Chapter 6 -A lab in a chamber - in situ methods in VP-ESEM and other applications 6.1 Introduction 6.2 Nanocharacterisation of insulating materials 6.3 In situ experiments 6.4 Other applications

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Product Details
EAN
9780470065402
ISBN
0470065400
Publisher
Other Information
Illustrated
Dimensions
15.8 x 2 x 23.6 centimeters (0.50 kg)

Table of Contents

Contents

Chapter 1 -A brief historical overview

1.1 Scanning electron microscopy

1.2 The development of imaging in a gas environment

Chapter 2 -Principles of SEM

2.1 Introduction

2.2 Electron sources

2.3 Electron optics

2.4 Signals and detection

2.5 Practical aspects of electron beam irradiation

2.6 the sem in operation

 

Chapter 3 -General principles of VP-ESEM: utilising a gas

3.1 Introduction

3.2 VP-ESEM instrumentation

3.3 Signal generation in a gas

3.4 Imaging with water vapour 

 

Chapter 4 -Imaging and analysis in the VP-ESEM: the influence of a gas

4.1 Introduction

4.2 Background to theoretical calculations 

4.3 Which gas?

4.4 Exploring the gas path length

4.5 How much gas?

4.6 X-ray microanalysis in the VP-ESEM

 

Chapter 5 -Imaging uncoated specimens in the VP-ESEM

 5.1 Introduction

5.2 Electronic structure

5.3 Factors affecting secondary electron emission

5.4 The influence of the specimen on the system

5.5 Time- and temperature-dependent effects

5.6 imaging soft materials

5.7 Effects of ions on imaging

5.8 Imaging with a gas: summary

 

Chapter 6 -A lab in a chamber – in situ methods in VP-ESEM and other applications

 6.1 Introduction

6.2 Nanocharacterisation of insulating materials

6.3 In situ experiments

6.4 Other applications

About the Author

Dr Debbie Stokes, Academic Visitor, Cavendish Laboratory, University of Cambridge, UK and Director of MicroSci; Obtained her degree in polymers from Bristol University in 1994.
In 1996 moved to Cavendish laboratory to do her Ph D on use of environmental SEM with Professor Athene Donald.
In 1999 became Royal Society Dorothy Hodgkin Research Fellow and a Junior Research Fellow of Newnham College, Cambridge, becoming a Senior Research Fellow in 2002.
Currently working at the Cavendish Laboratory funded by her consultancy business MicroSci.

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